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With the silicon powder and the metal tantalum, crush the silicon and put it into a graphite oven for heating to 1100-100-1500. Then pass through to the hydrogen. Finally, heating to 800 will result in tantalum silicate. You can also reduce tantalum peroxide with calcium hydroxide and make tantalum hydride. Then heat 1800 tantalum metallic to produce tantalum silicate. For the second type of reaction, the Si/Ta mixture was heated to 350 degrees before being heated to 1480. You can also allow TaS2 reaction with SiHnX4N to occur at 900 Direct is the third option. As follows, tantalum powder and silicon powder are combined to make Tantalum Silicate. To prepare tantalum silicate, first crush and mix the silicon powder with metal tantalum. Then heat to 1100 1500 for pre-reaction. After the injection of hydrogen, it is heated up to 1800°C for a homogenization process for 1 h. This will produce tantalum silicate. Fourth tantalum pentoxide reduction process: first reduce the calcium with hydroxide to get tantalum hydrochloride. Next, heat tantalum to 1800 and add silicon powder to create tantalum silicate.
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